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Friday 11/1/2018


Synthesis 1 (AS02) 1 from 0 (attempt 2)

Today I started the synthesis of 1 from 0. The details were:

In a 50 mL two neck round bottom flask, 101.6 mg of 0 was dissolved in 20 mL of acetic acid. With constant stirring, 86 mg of hexylamine (\(\ce{H2N-C6H13}\)) was added dropwise to the acetic acid. The flask was then capped and refluxed at 120\(^\circ\) C$ for two hours before being removed from the heat off and left at room temperature with stirring over the weekend.


  • TLC was not run, as acetic acid is very polar and prevents the rest of the compounds from migrating individually.