Skip to content

XRD

  • XRD is the process by which reflected X-Rays interfere with each other when reflected off the different layers within a crystal
  • The general rule is that \(n\lambda=2sin\theta\), which relates the distance between the two layers reflecting the xrays to the wavelength of the xrays bombarding the crystal.

image

  • XRD can be used to analyse both a single crystal and a crystalline powder.
  • Since the orientation of the crystals can’t be aligned in a powder, the resulting diffraction pattern becomes a series of concentric circles.
  • Single crystal spectra can be used to determine the absolute structure of a unit cell, and therefore the molecule
  • Powder diffraction is used more as a profiling/fingerprinting technique

image